Chemical and Biological Engineering ETDs

Publication Date

Summer 7-15-2025

Abstract

This dissertation develops and validates a semi-empirical Flory–Huggins-based interaction model, combined with Cahn–Hilliard simulations, for predicting multi-component liquid–liquid phase separation (LLPS) in elastin-like polypeptide (ELP) systems. Equilibrium droplet compositions, measured using a PDMS-based microfluidic device, enabled direct parameterization of interaction coefficients. The model was applied to generate phase diagrams and assess composition dependence in ternary mixtures. Cahn–Hilliard simulations were conducted to explore potential phase morphologies under different interfacial conditions. Multi-component Lattice Boltzmann simulations were implemented to model droplet morphology evolution under varying interfacial and diffusive parameters, reproducing experimentally relevant morphologies. A three-phase wetting study revealed conditions for selective wetting and phase encapsulation, with implications for multi-phase compartment design. These results collectively establish a quantitative link between experimentally accessible parameters and predictive phase behavior in ELP mixtures, offering a platform for rational engineering of multi-phase condensates.

Keywords

Lattice Boltzmann Method, Liquid-Liquid Phase Separation, Cahn-Hilliard, Flory-Huggins, interfacial dynamics

Document Type

Dissertation

Language

English

Degree Name

Chemical Engineering

Level of Degree

Doctoral

Department Name

Chemical and Biological Engineering

First Committee Member (Chair)

Nichlaus J. Carroll

Second Committee Member

Gabriel P. Lopez

Third Committee Member

Dimiter N. Petsev

Fourth Committee Member

Alexander Wagner

Comments

The material in this dissertation is based upon work supported by the National Science Foundation under grant numbers CBET-2048051 and EF-2318897 along with the Graduate Research Fellowship Program DGE-1939267. The opinions and conclusions contained herein are those of the author and not necessarily that of the NSF's.

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